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溶剂萃取/溶剂辅助风味蒸发-气相色谱/质谱联用分析野韭菜花挥发性成分 被引量:22

Analysis of Volatiles in Wild Chinese Chive Flowers by Solvent Extraction/Solvent-Assisted Flavor Evaporation Coupled with Gas Chromatography-Mass Spectrometry
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摘要 以乙醚为溶剂,采用溶剂萃取/溶剂辅助风味蒸发法(solvent extraction/solvent-assisted flavor evaporation,SE/SAFE)提取新鲜野韭菜花精油,采用气相色谱-质谱联用(gas chromatography/mass spectrometry,GC-MS)法结合双柱(RTX-5色谱柱和DB-WAX色谱柱)保留指数(retention index,RI)定性分析精油中的挥发性成分。结果共鉴定出47种挥发性成分,其中包括含硫化合物28种、醛类4种、醇类3种、酮类3种、烃类化合物9种。含硫化合物数量多且含量大,是新鲜野韭菜花中的主要挥发性成分。 The essential oil in fresh flowers of wild Chinese chive was extracted by solvent extraction/solvent-assisted flavor evaporation(SE/SAFE) and analyzed by gas chromatography-mass spectrometry(GC-MS) carried out on the non-polar capillary column RTX-5 and the polar capillary column DB-WAX,respectively based on retention index(RI).Totally 47 compounds were identified,including 28 sulfur-containing compounds,4 aldehydes,3 alcohols,3 ketones and 9 hydrocarbons.The major volatiles of fresh flowers of wild Chinese chive were sulfur-containing compounds.
出处 《食品科学》 EI CAS CSCD 北大核心 2011年第20期211-216,共6页 Food Science
基金 国家"863"计划项目(2011AA100903) 北京市属高等学校人才强教计划项目(PHR20090504)
关键词 新鲜野韭菜花 溶剂萃取/溶剂辅助风味蒸发 气相色谱-质谱联用 挥发性成分 fresh wild Chinese chive flowers solvent extraction/solvent-assisted flavor evaporation(SE/SAFE) gas chromatography-mass spectrometry(GC-MS) volatiles
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参考文献16

  • 1吴莉,陈文利.韭叶中化学成分的生物活性研究[J].化学与生物工程,2005,22(2):49-51. 被引量:16
  • 2TAKAHASHI M, SHIBAMOTO T. Chemical compositions and anti- oxidant/andin ammatory activities of steam distillate from freeze-dried onion (Allium cepa L.) sprout[J]. Journal of Agricultural and Food Chemistry, 2008, 56(22): 10462-10467.
  • 3吴莉,张平.韭菜中香味成分的最佳检测条件的研究[J].化工时刊,2005,19(7):29-31. 被引量:10
  • 4NIELSEN G S, POLL L. Determination of odor active aroma com- pounds in freshly cut leek (Allium ampeloprasum var. bulga) and in long-term stored frozen unblanched and blanched leek slices by gas chromatography olfactometry analysis[J]. J Agric Food Chem, 2004, 52.
  • 5ENGEL W, BAHR W, SCHIEBERLE P. Solvent assisted flavour evaporation-a new and versatile technique for the careful and direct isola- tion of aroma compounds from eomple food matrices[J]. Eur Food Res Technol, 1999, 209(3/4): 237-241.
  • 6穆启运.细叶韭花化学成分的研究[J].西北植物学报,2001,21(6):1204-1208. 被引量:22
  • 7BLOCK E, NAGANATHAN S, PUTMAN D, et al. Allium chemistry: HPLC analysis of thiosulfmates from onion, garlic, wild garlic (ramsom), leek, scallion, shallot, elephant (great-headed) garlic, chive, and Chinese chive. Uniquely high allyl to methyl ratios in some garlic samples[J]. Journal of Agricultural and Food Chemistry, 1992, 40(12): 2418-2430.
  • 8MONDY N, DUPLAT D, CHRISTIDES I, et al. Aroma analysis of fresh and preserved onions and leek by dual solid-phase microextration-liquid extraction and gas chromatography-mass spectrometry[J]. Journal of Chromatogrtaphy A,2002,903(1/2):89-93.
  • 9卫煜英,曹艳平,李延墨,冷毅.韭菜花挥发性成分的气相色谱-质谱分析[J].色谱,2003,21(1):96-96. 被引量:48
  • 10KREST I, GLODEK J, KEUSGEN M. Cysteine sulfoxides and alliinase activity of some Allium species[J]. J Agric Food Chem, 2000, 48(8): 3753-3760.

二级参考文献17

  • 1刘美筠,万仁忠,王建华.韭菜精油的研究[J].山东农业大学学报(自然科学版),1993,24(3):323-327. 被引量:6
  • 2卫煜英,万仁忠.韭菜挥发油主要成份的气相色谱/质谱分析[J].分析化学,1996,24(2):192-194. 被引量:20
  • 3张世琏,吴莉,杨光忠.韭菜中挥发性含硫组分的GC/MS研究[J].华中师范大学学报(自然科学版),1996,30(2):182-185. 被引量:14
  • 4孟正木,王佾先,操燕明,纪江.草钟乳挥发性成分的研究[J].中国药科大学学报,1996,27(3):139-140. 被引量:10
  • 5中国科学院兰州沙漠研究所.中国沙漠植物志(二)[M].北京:科学出版社,1987.249-249.
  • 6中国植物志编辑委员会.中国植物杂志(第14卷)[M].北京:北京科学出版社,1980.170-170.
  • 7朱建设 见 卢佩章 张玉奎.第九次全国色谱学术报告会文集[M].沈阳:辽宁科学技术出版社,1993.265.
  • 8郭海忱 王玲 唐非 崔兰 周秀清.质谱学报,1988,9:41-41.
  • 9中国饲用植物志编辑委员会.中国饲用植物志(第一卷)[M].北京:农业出版社,1987.528-539.
  • 10Block Eric, Putman David, Zhao shuhai. Allium chemistry: GC/MS analysis of thiosulfinates and related compounds from onion, leek,scallion, shallot, chive and chinese chive [ J ]. J. Agric . Food Chem,1992,40 (12) :2431 - 2438.

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