摘要
Key intermediate bis[2-amino-4,5-(15-crown-5)phenyl]diselenide was obtained by the convenient redox method. Crown-ether type host molecule containing Se-Se bond 2,11-dioxo-4,5:8,9-di(benzo[4',5']-15-crown-5)-6,7-diselena-3,10,16-triazabicyclo[10,3,1]hexadeca-1(16), 4, 8, 12, 14-pentaene was synthesized with high dillution technique.
Key intermediate bis[2-amino-4,5-(15-crown-5)phenyl]diselenide was obtained by the convenient redox method. Crown-ether type host molecule containing Se-Se bond 2,11-dioxo-4,5:8,9-di(benzo[4',5']-15-crown-5)-6,7-diselena-3,10,16-triazabicyclo[10,3,1]hexadeca-1(16), 4, 8, 12, 14-pentaene was synthesized with high dillution technique.