摘要
Ball milling induced microstructure evolution in an FeMoSiB alloy with three kinds of different phase constitutions (bcc alpha -Fe solid solution and various borides) was investigated by means of X-ray diffraction and transmission electron microscopy. Experimental evidences indicate that a same final product of bcc alpha -Fe solid solution is formed upon milling for all samples. During the transformation, the XRD peaks of alpha -Fe phase shift to lower diffraction angles, and those of borides disappear in turn, first the metastable Fe//3B and Fe//2//3B//6 and then the stable Fe//2B. The observed structural evolution might originate from the transformation of ordered Fe//2B phase into disordered alpha -Fe solid solution. (Edited author abstract) 8 Refs.
Ball milling induced microstructure evolution in an FeMoSiB alloy with three kinds of different phase constitutions (bcc alpha -Fe solid solution and various borides) was investigated by means of X-ray diffraction and transmission electron microscopy. Experimental evidences indicate that a same final product of bcc alpha -Fe solid solution is formed upon milling for all samples. During the transformation, the XRD peaks of alpha -Fe phase shift to lower diffraction angles, and those of borides disappear in turn, first the metastable Fe//3B and Fe//2//3B//6 and then the stable Fe//2B. The observed structural evolution might originate from the transformation of ordered Fe//2B phase into disordered alpha -Fe solid solution. (Edited author abstract) 8 Refs.