α-Oxoketene Cyclic S,S-Acetals Chemistry──Reaction of α,α′-Dioxo (ester)ketene Cyclic S,S-Acetals with Ethylenediamine
oroxoketene Cyclic S,S-Acetals Chemistry ──Reaction of α, α′ -Dioxo (ester )ketene Cyclic S,S-Acetals with Ethylenediamine
摘要
α, α′ -Dioxo (ester ) ketene cyclic S, S-acetais 2 were reacted withethyleneddriine to chrd α, α′-dioxo (ester)ketene cyclic N, N-acetals 3 Thisprocess provides a new method for the synthesis of 3 in gnd yteld under mildcondition. All products are confirmed with elementai analpeis, IR, 1H NMR and13~C NMR
α, α′ -Dioxo (ester ) ketene cyclic S, S-acetais 2 were reacted withethyleneddriine to chrd α, α′-dioxo (ester)ketene cyclic N, N-acetals 3 Thisprocess provides a new method for the synthesis of 3 in gnd yteld under mildcondition. All products are confirmed with elementai analpeis, IR, 1H NMR and13~C NMR
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1Mei Xin ZHAO,Qun LIU,Fu Shun LIANG,Jing Fu LIU,Bao Zhong ZHAO,LianZhong LI,(Department of Chemistry, Northeast Normal University, Changchun, 130024)(Department of Chemistry, Jilin Teacher college, Jilin, 131000).α-Oxoketene Cyclic S, S-cetals Chemistry-Substitution Reaction of α,α'-Dicinnamoyl Ketene Cyclic S, S-Acetals with Ethylenediamine[J].Chinese Chemical Letters,1998,9(3):231-232. 被引量:2
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2Han Song CHEN,Zheng Ming LI,Zhong Wen WANG (State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry Nankai University, Tianjin 300071).A Convenient Synthesis of Pyrazolylpyrazoles Using α-Oxo Ketene S,S- and N,S-Acetals[J].Chinese Chemical Letters,1999,10(8):643-646.
-
3Zhi Tang HUANG Ping Cheng ZHANG Institute of Chemistry,Academia Sinica,Beijing,100080.SYNTHESIS AND TAUTOMERISM OF KETENE N,O-ACETALS WITH BENZOXAZOLINE RING[J].Chinese Chemical Letters,1990,1(2):167-170.
-
4赵丽薇,阚伟,于海涛,付宏刚,孙家钟.Theoretical Study on the Reaction Mechanism of Ketene CH2CO with Isocyanate NCO Radical[J].Chinese Journal of Chemistry,2007,25(8):1105-1111.
-
5Mang WANG,Qun LIU,Mei Xing ZHAO,Li Min WANG (Department of Chemistry, Northeast Normal University, Changchun 130024).Intramolecular Aldol Condensation ofα- Oxo Ketene Dibenzylthioacetals: A Facile Route to Substituted Thiophenes[J].Chinese Chemical Letters,2000,11(1):3-4.
-
6Shu Jia ZHANG,Ji Geng TANG,Qun LIU(Department of Chemistry, Northeast Normal University.Changchun, 130024)Yan XING,Yong Hua LIN(Changchun Institute or Applied Chemistry, Academy of Science,).THE CRYSTAL STRUCTURE AND STEREOCHEMISTRY OF BENZOYL KETENE O,S ETHYLENE ACETAL[J].Chinese Chemical Letters,1994,5(12):1031-1032.
-
7Zai Ming ZHU,Yong Ting XU(Department of chemistry, Liaoning NOrmal University,Delian, 116029)Qun LIU(Department of Chemistry,Northeast Normal University,Changchun, 130024)Jie Han HU(Dalian Institute of Chemical Physics,Academia Sinica,Dalian, 116001).α-OXOKETENE CYCLIC DITHIOACETALS CHEMISTRY ──REACTION OF α,α-DIOXO(ESTER)KETENE CYCLIC DITHIOACETALS WITH BUTANONE[J].Chinese Chemical Letters,1996,7(2):95-98.
-
8Li, JX,Liu, Q,Zhao, MX,Liu, JF,Li, SY,He, Y.Synthesis of Triphenyltin 2-(1,2-Ethylenedithio) Methylene-3-Oxo-5-Aryl-4-Pentenoate[J].Chinese Chemical Letters,1998,9(1):21-22.
-
9Chen, K,Yang, HZ.Stepwise Oxidation of Ketene Dithioacetal[J].Chinese Chemical Letters,2001,12(10):865-868.
-
10Qun LIU,Zhi Ling WANG,Shu Jia ZHANG,Zhi Yun YANG(Department of Chemistry, Northeast Normal University, Changchun, 130024).STUDIES ON THE REACTIVITY OF CYCLOAROMATIZATION REACTION VIA a-OXO KETENE DITHIOACETALS[J].Chinese Chemical Letters,1994,5(7):577-580.