Studies on Silicon-Containing Fragrance Raw Materials(Ⅳ)——Synthesis of Spiro-Acetals of 5-Trimethylsilylcyclohex-2-(or 3)enone

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摘要 Some novel spiro-acetals of 5-trimethylsilylcyclohex-2(or 3)-enone were synthesized from the reaction of silylcyclohexenones with the corresponding a, ω-diols in the presence of oxalic acid or adipic acid. Some novel spiro-acetals of 5-trimethylsilylcyclohex-2(or 3)-enone were synthesized from the reaction of silylcyclohexenones with the corresponding a, ω-diols in the presence of oxalic acid or adipic acid.

作者 TANG Shi-xiong XUE Jie-you DUAN Mao-sheng CAO Yu-rong ZHI Jing-fang WANG Xiao-lan

机构地区 Department of Chemistry

出处《Chemical Research in Chinese Universities》 SCIE CAS CSCD 1993年第2期127-132,共6页 高等学校化学研究（英文版）

基金 Supported by NSFC and Youth Foundation of Tianjin

关键词 Synthesis 5-trimethylsilylcyclohex-2(or 3)-enone Spiro-acetal

分类号 O6 [理学—化学]

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1TANG Shi-xiong, XUE Jie-you, DUAN Mao-shengCAO Yu-rong, ZHI Jin-fang and WANG Xiao-Ian(Department of Chemistry, Nankai University, Tianjin, 300071).Studies on Silicon-Containing Fragrance Raw Materials( Ⅲ )——The Addition of 5-Trimethylsilylcyclohex-3-enone with Grignard Reagent[J].Chemical Research in Chinese Universities,1993,9(1):40-44.
2TANG Shi-xiong, XUE Jie-you, WU Jun-jun, CAO Yu-rongZHI Jin-fang WANG Xiao-lan (Department of Chemistry, Nankai University, Tianjin, 300071).Studies on Silicon-Containing Fragrance Raw Materials( Ⅱ )——Syntheses and Odors of 4-Trimethylsilylcyclohex-3-enol and 4-Trimethylsilylcyclohexanol Derivatives[J].Chemical Research in Chinese Universities,1993,9(2):121-126.
3Tang Shixiong, Liu Hong, Wang Changfeng, Cao Yurong, Liao Xiangmin and Wang Xiaolan (Department of Chemistry, Nankai University, Tianjin).Studies on Fragrance Raw Materials of α-Terpineol Analogues[J].Chemical Research in Chinese Universities,1991,7(4):212-220. 被引量：1
4欧阳小月,江焕峰,黄精美.A Facile Method for the Epoxidation of Cyclic Enone Catalyzed by tert-BuNH2 with 30% Hydrogen Peroxide as Oxidant[J].Chinese Journal of Chemistry,2006,24(10):1480-1482.
5M.M.Campbell,D.W.Brown.STUDIES ON CYCLOPENT-2-ENONE: (Ⅲ) THE STUDY ON DECONJUGATION OF CYCLOPENT -2-ENONE ALDOL ADDUCTS[J].Chinese Chemical Letters,1991,2(10):777-780.
6LI Yang-xue XUE Ming HUANG Lin CHEN Si-ru QIU Shi-lun.Synthesis, Structures, Fluorescence and Magnetism of Two Lanthanide Metal-organic Frameworks with CaF2 Topology Based on Silicon-centered Tetrahedral Ligand[J].Chemical Research in Chinese Universities,2013,29(4):611-616.
7LI Yang-xue XUE Ming GUO Li-jia HUANG Lin CHEN Si-ru QIU Shi-lun.Syntheses, Structures, Fluorescence and Magnetism of Six Lanthanide Metal-organic Frameworks Based on Silicon-centered Tetrahedral Ligand[J].Chemical Research in Chinese Universities,2013,29(2):196-200. 被引量：4
8Shu Jia ZHANG,Ji Geng TANG,Qun LIU(Department of Chemistry, Northeast Normal University.Changchun, 130024)Yan XING,Yong Hua LIN(Changchun Institute or Applied Chemistry, Academy of Science,).THE　CRYSTAL　STRUCTURE　AND　STEREOCHEMISTRY　OF　BENZOYL　KETENE　O，S　ETHYLENE　ACETAL[J].Chinese Chemical Letters,1994,5(12):1031-1032.
9Ji Mao LIN,Hui ZHANG,Ai You HAO,Qin Zheng YANG(Department of Chemistry, Shandong University, Jinan, 250100).Elimination Reaction of α,ω-Diols by Magnesium[J].Chinese Chemical Letters,1998,9(8):697-698.
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Chemical Research in Chinese Universities

1993年第2期

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Studies on Silicon-Containing Fragrance Raw Materials(Ⅳ)——Synthesis of Spiro-Acetals of 5-Trimethylsilylcyclohex-2-(or 3)enone

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