摘要
The title compound was synthesised and the X-ray diffraction analysis shows that the crystal belongs to in monoclinic system, space group P21/n with α=16. 972(4) A ,b=14. 128(3)A , c = 22. 615(4)A ,β=103.16(2)°,V=528.14A3,F(000) = 2264, Z=4. Both cation [YQ(HQ)2]2+ and anion [NiQ3]- are of distorded octahedral geometry with coordination number of 6. Its IR spectrum was recorded.
The title compound was synthesised and the X-ray diffraction analysis shows that the crystal belongs to in monoclinic system, space group P21/n with α=16. 972(4) A ,b=14. 128(3)A , c = 22. 615(4)A ,β=103.16(2)°,V=528.14A3,F(000) = 2264, Z=4. Both cation [YQ(HQ)2]2+ and anion [NiQ3]- are of distorded octahedral geometry with coordination number of 6. Its IR spectrum was recorded.
