摘要
主要介绍了有机加合物C10H11NO8的合成及结构研究。采用缓慢蒸发溶剂法合成了有机加合物单晶体,该加合物通过红外、热化学和X-射线单晶衍射分析方法确证。X-射线单晶衍射分析显示,晶体中分子主要依靠分子间氢键相互连接,在晶体中构成了氢键网络。对该加合物分子的微观晶体结构进行了讨论。
An organic adduct C10H11NO8 was synthesized and the crystal structure was measured.Through the use of slow solvent evaporation synthesis of single crystal organic adduct.The adduct analysis by infrared and thermal chemical analysis,X-ray diffraction analysis showed that the crystal mainly depends on the molecular hydrogen bonds between the molecules connected in the crystal constitutes a hydrogen bond network.The adduct crystal structure of the micro-elements are discussed.
出处
《化学试剂》
CAS
CSCD
北大核心
2011年第12期1073-1076,共4页
Chemical Reagents
基金
国家自然科学基金资助项目(21065012)
2010年科技支疆项目(201091244)
关键词
合成
氢键
加合物
晶体结构
synthesis
hydrogen bond
adduct
crystal structures
