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4-正丁基-3,4-二氢-1H-噻吩并[2,3-e][1,4]-二氮杂卓-2,5-二酮的合成 被引量：1

Synthesis of 4-butyl-3,4-dihydro-1H-thieno[2,3-e][1,4]diazepine-2,5-diones
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摘要 以氰基乙酸乙酯为起始原料,经4步反应得到目标化合物4-正丁基-3,4-二氢-1H-噻吩并[2,3-e][1,4]-二氮杂卓-2,5-二酮,反应条件温和,后处理简单.经红外、核磁分析,所得数据与其结构相吻合. Novel compounds,4-butyl-3,4-dihydro-1H-thieno[2,3-e][1,4]diazepine-2,5-dioneswere synthesized using ethyl cyanacetate as initial material after a 4-step reaction,with mild reactionconditions and simple post treatment.The structure of the target molecules were detected by IR and1 H NMR,and the spectrum results were consistent with the molecular structure.
作者 苏杭 何西平 张丽 卢翠芬 杨桂春
机构地区 湖北大学化学化工学院
出处 《湖北大学学报（自然科学版）》 CAS 北大核心 2011年第4期501-504,共4页 Journal of Hubei University：Natural Science
基金 湖北省自然科学基金重点项目(2008CDA078)资助
关键词 噻吩 二氮杂卓 合成 thiophene diazepine synthesis
分类号 O622.6 [理学—有机化学]
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湖北大学学报（自然科学版）
2011年 第4期

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