9-(2-苯并咪唑基)壬酸盐酸盐水合物的晶体结构

Crystal Structure of 9-(1H-benzo[d]imidazol-2-yl)nonanoic acid chloride hydrate

以邻苯二胺和1,10-癸二酸为原料,在4 mol/L盐酸中反应制备新化合物9-(2-苯并咪唑基)壬酸盐酸盐水合物,利用X-射线衍射法测定其晶体结构。晶体数据:单斜晶系,空间群P21/c,a=0.80033(12)nm,b=4.2375(6)nm,c=0.52327(8)nm,α=90°,β=91.170(5)°,γ=90°,V=1.7742(5)nm3,Z=4。

9-（1H-benzo[d]imidazol-2-yl）nonanoic acid chloride hydrate as a novel compound was prepared in a solution of 4M HCl through the material of o-phenylenedimine and 1,10-decanedicarboxylic acid.The title compound was characterized by single X-ray diffraction,crystal data for title compound： L：monochnic,space group P21/c,a=0.80033（12） nm,b=4.2375（6） nm,c=0.52327（8） nm,α=90°,β=91.170（5） °,γ=90°V=1.7742（5） nm3,Z=4.