跌打伤科酒质量标准分析与研究

Study on The quality standard for Dieda shangke Jiu

目的为了更好的控制跌打伤科酒的产品质量,建立相关药材的薄层色谱鉴别和高效液相含量测定。方法采用薄层色谱法,对泽兰和两面针二味药材进行薄层鉴别;用高效液相法,对徐长卿药材中的丹皮酚进行含量测定。结果鉴别方法:操作简单,专属性强,阴性对照无干扰;含量测定方法:操作简单,准确,丹皮酚在1.9266～123.3000g之间呈良好的线性关系,丹皮酚的回收率为98.44%。结论方法简便,结果可靠,对跌打伤科酒质量标准的分析与研究提供科学的依据。

Objective In order to control the quality of Dieda shangke Jiu,we establish TLC method for identification and HPLC method for content determination of relevant Chinese herbal medicines.Methods Use TLC methods for identification of Herba Lycopi and Radix Zanthoxyli,used HPLC method for content determination of paeonol in Herba Lycopi.Results The TLC methods we established were simply,steady and selectine.The HPLC method we established was simply,accurate and had a good linearity in the range of 1.9266～123.3000μg,with a mean recovery of paeonol as high as 98.44%.Conclusion The methods we established are easy and accurate.This quality standard can control the quality of Dieda shangke Jiu.