摘要
A 0.7 mm-thick wavy γ-TiAl sheet with fully lamellar microstructure was fabricated by hot pressing Ti/Al alternate foils with heat treatment of 640 °C, 15 h+850 °C, 35 h+1350 °C, 2 h. The intermetallic compounds formed during heat treatments were identified by scanning electron microscopy (SEM) and X-ray diffraction (XRD). TiAl3 was the only observed phase at the Ti/Al interface when Al foils were not consumed. After being annealed at 850 °C for 35 h, the microstructure was composed of α-Ti, α2-Ti3Al, γ-TiAl and TiAl2. A fully lamellar microstructure formed after annealing at 1350 °C. Most of the angles between the lamellar interface and the sheet plane are below 30°. Using thinner starting foils is favorable to produce sheets with fine microstructure.
用热压逐层叠置的Ti/Al箔的方法制备具有全片层结构的γ-TiAl波纹板。热处理工艺为640°C,15h+850°C,35h+1350°C,2h。用扫描电镜(SEM)和X射线衍射(XRD)分析热处理过程中产生的金属间化合物相。在Al箔完全消耗之前,Ti/Al界面仅有TiAl3相生成。在850°C热压35h后,基体由α-Ti,α2-Ti3Al,γ-TiAl和TiAl2相组成。冷却得到全片层结构,大部分片层与板面的夹角小于30°。采用较薄的原料箔可以获得相对细小的微观组织。
基金
Project (50771041) supported by the National Natural Science Foundation of China
Project (05-0350) supported by the New Century Excellent Talents in University, China