三嗪类环蕃的合成与表征

Synthesis and characterization of heterocyclophanes containing 1,3,5-triazine

以三聚氯氰、乙胺、二甲胺、甲胺、苯酚、二(4-氨基苯基)甲烷等为原料,经取代、傅克反应和成环反应,合成了一类新型三嗪类杂环蕃(4a,4b,4c),并通过1H NMR、IR和MALDI-TOF-MS对其结构进行了表征。

Some novel heterocyclophanes containing 1,3,5-triazine（4a,4b,4c） were synthesized from cyanuric chloride,ethylamine,dimethylamine,aniline,phenol and di（4-aminophenyl）methane by substitution,Friedel-Crafts alkylation and cyclization.The structures were characterized by 1H NMR,IR and MALDI-TOF-MS methods.