酞菁钇固相法合成与表征

Synthesis and characterization of phthalocyanine ytrium by solid-state reaction

本文以苯酐、尿素、稀土金属盐、钼酸铵为原料,采用固相合成法合成新型酞菁钇配合物,摸索其适宜反应路线,并采用红外光谱对其主要官能团进行表征。

Metallophthalocyanines are known not only as classical dyes in practical use but also as modern functional materials. However, detailed preparation of yttrium phthalocyanine wasn＇t reported up to the present. In this paper, yttrium phthalocyanine was synthesized by the solid reaction of urea, phthalie anhydride, molybdic ammonium with hydrate nitric acid yttrium using carbonate sodium as catalyzer. The strueture was verified by IR.