摘要
诺卜醇经Ni(R)催化氢化合成氢化诺卜醇,氢化诺卜醇与7种羧酸进行酯化反应合成7种羧酸酯,产率均在90%以上,GC纯度达98%.对合成的羧酸酯均进行了IR、1H NMR、13C NMR与MS分析。
Hydronopol was prepared from the hydrogenation of nopol in the presence of Raney Ni. And hy- dronopol reacts with 7 different kinds of carboxylic acids to produce new compounds of hydronopyl carboxylic ether series. The yield of the products （GC content were over 98%） were not less than 90%. Identification and structural analysis were done using IR, 1H NMR, 13C NMR and MS methods.
出处
《江西师范大学学报（自然科学版）》
CAS
北大核心
2012年第1期12-15,共4页
Journal of Jiangxi Normal University(Natural Science Edition)
基金
国家自然科学基金(30860223
31060101)
教育部留学回国人员科研启动基金([2010]1561)
江西省青年科学家(井冈之星)培养对象计划资助项目
关键词
诺卜醇
氢化诺卜醇
催化氢化
酯化
结构分析
nopol
hydronopol
catalytic hydrogenation
esterification
structural analysis
