摘要
以邻溴苯胺为原料,经过酰化、烯丙基化,最后在Pd配体催化下经Heck反应得到目标产物N-苯甲酰基-3-甲基吲哚,最后采用IR,1 H NMR和13 C NMR等手段对目标产物的结构进行确认。
N-Benzoyl-3-Methyl-Indoline was prepared from 2-bromoaniline through acylation and allylation, followed by Heck reaction using Pd as catalyst. The target compound was verified by several methods,suchas IR,^1H NMR and ^13C NMR.
出处
《南昌大学学报(理科版)》
CAS
北大核心
2012年第1期47-49,共3页
Journal of Nanchang University(Natural Science)
基金
江西省自然科学基金资助项目(2010ZH0104)