N-苯甲酰基-3-甲基吲哚的合成及表征

Synthesis and characteristics of N-Benzoyl-3-Methyl-Indoline

以邻溴苯胺为原料,经过酰化、烯丙基化,最后在Pd配体催化下经Heck反应得到目标产物N-苯甲酰基-3-甲基吲哚,最后采用IR,1 H NMR和13 C NMR等手段对目标产物的结构进行确认。

N-Benzoyl-3-Methyl-Indoline was prepared from 2-bromoaniline through acylation and allylation, followed by Heck reaction using Pd as catalyst. The target compound was verified by several methods,suchas IR,^1H NMR and ^13C NMR.