摘要
本文以顺丁烯二酸酐、氯苯经Friedle-Crafts反应合成了1,2-二(4-氯苯甲酰基)乙烯。经Diels-Alder反应,以异戊二烯环加成合成了含环己烯结构的双氯双酮化合物:1-甲基-4,5-二(4-氯苯甲酰基)环己烯。该氯代双酮化合物具有不饱和双键结构,是制备聚芳醚酮功能高分子材料的理想单体。
A novel compound, the 1 - methyl-4, 5-bis(4-chlorobenzoyl) cyclohexen containing cycohexene was prepared. The compound was analysed by MS FT-IR, 1H-NMR, 13C-NMR and Dept 135. It has been proved that compound was the monomer of functional polymers.
出处
《染料工业》
2000年第1期25-26,28,共3页
Dyestuff Industry
基金
国家自然科学基金(59473019)