1,1'-双[(二苯膦)甲基]二茂铁的合成

Synthesis of 1,1'-bis[(diphenylphosphino)methyl]ferrocene

对1,1’双[(二苯膦)甲基]二茂铁的合成路线进行了设计,详细报导了其合成方法,筛选了反应工艺条件,讨论了影响反应的各种因素。对最终产物和中间物进行了红外测试,并对红外谱图进行了解析。结果表明所设计的合成路线合理可行。

A new synthesis route for 1,1' bis[(diphenylphosphino)methyl]ferrocene(DPMF)was designed. The preparation method of DPMF and the influences of various factors on the reactions were also discussed in detail. The product was characterized by IR spectroscopy. The result shows that the synthesis route and preparation method is reasonable.