摘要
从刺山柑果实中首次分离纯化得到S8单质。经X-射线单晶衍射分析,确认该化合物为S8晶体,M=256.48。晶体属斜方晶系,空间群Fddd。晶胞参数a=10.456(7),b=12.908(9),c=24.483(17),V=3305(4)3,Z=16,F(000)=2048,R1=0.0915,wR2=0.1820。
The purpose of this paper studied single crystal structure of S8 isolated firstly from Capparis spinosa fruits.The S8 crystal structure was investigated by single-crystal X-ray crystallographic analysis crystallizes in the monoclinic system,M=256.48.space group Fddd.Unit cell parameters a=10.456（7）,b=12.908（9）,c=24.483（17）,V=3305（4）3,Z=16,F（000）=2048.The final R1=0.0915,wR2=0.1820.
出处
《广西植物》
CAS
CSCD
北大核心
2012年第2期257-260,共4页
Guihaia
基金
Supported by Policy Guiding Project of Science and Technology Bureau of Xinjiang Production and Construction Corps(2006YD29)
Open Project of Xinjiang Prodution and Constrction Key Laboratory of Protection and Utilization of Biological Resources in Tarim Basin(BR0609)
关键词
刺山柑
硫单质
X-射线单晶衍射
晶体结构
Capparis spinosal
element sulfur
single-crystal X-ray diffraction
crystal structure
