摘要
目的:建立内在质量监控指标,提高药品质量标准。方法:采用气相色谱法测定丁香酚的含量。结果:丁香酚在40ng～400ng范围内呈良好线性关系,回归方程Y=1387.6X-2812.2 R=0.9995,平均回收率为99.78%,RSD为0.62%。结论:该方法简便、灵敏、准确,可用于红花清肝十三味丸的内在质量监控。
Objective：Build an internal quality control guideline to improve medicine quality standard.Method：Apply gas chromatography method to get eugee content determination.Result：Between 40ng^400ng,eugee shows a linear relation,regression equation is Y=1387.6X-2812.2 R=0.9995,average recovery is 99.78%,RSD is 0.62%.Conclusion：The method is easy to apply and with accuracy and sensitivity,which can be applied in internal quality control of Safflower Removing Liver-fire Pill of Thirteen Ingredients.
出处
《内蒙古医学院学报》
2012年第1期65-68,共4页
Acta Academiae Medicinae Neimongol
基金
内蒙古自治区卫生厅(200614)
关键词
红花清肝十三味丸
气相色谱法
丁香
丁香酚
含量测定
Safflower Removing Liver-fire Pill of Thirteen Ingredients
Gas chromatography
Clove
Eugee
Content Determination
