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Separation of arenols from a high-temperature coal tar 被引量:3

Separation of arenols from a high-temperature coal tar
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摘要 A high-temperature coal tar collected from Xuzhou Coking Plant,Saint-Gobain Pipelines(Xuzhou) Co.,Ltd.was exhaustively extracted with petroleum ether(PE).The extract was sequentially eluted through silica gel with PE and PE/ethyl acetate(EA) mixed solvents(volume ratio 2:1) to afford two eluted fractions.The extract and eluted fractions were analyzed with gas chromatography/mass spectrometry.In total,14 arenols were detected,including phenol,cresols,xylenols,fluorenols,phenanthren-3-ol and pyren-1-ol. A high-temperature coal tar collected from Xuzhou Coking Plant, Saint-Gobain Pipelines (Xuzhou) Co., Ltd. was exhaustively extracted with petroleum ether (PE). The extract was sequentially eluted through silica gel with PE and PE/ethyl acetate (EA) mixed solvents (volume ratio 2:1 ) to afford two eluted frac- tions. The extract and eluted fractions were analyzed with gas chromatography/mass spectrometry. In total, 14 arenols were detected, including phenol, cresols, xylenols, fluorenols, phenanthren-3-ol and pyren-l-ol.
出处 《International Journal of Mining Science and Technology》 2012年第2期243-244,共2页 矿业科学技术学报(英文版)
基金 subsidized by the Fund from the Natural Science Foundation of China for Innovative Research Group (Grant50921002) the Priority Academic Program Development of Jiangsu Higher Education Institutions
关键词 高温煤焦油 油分离 气相色谱/质谱法 混合溶剂 乙酸乙酯 焦化厂 PE 石油醚 Coal tarArenolsColumn chromatographyIdentificationGC[MS analysis
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