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降脂宁颗粒挥发油成分的GC-MS分析

GC-MS Analysis of Volatile Oil Constituents of Jiangzhining Granules
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摘要 研究降脂宁颗粒挥发油的化学成分。采用中国药典一部(2010版)附录XD挥发油测定法对降脂宁颗粒的挥发油进行提取,用GC-MS对化学成分进行鉴定,以毛细管柱进行分析,面积归一化法测定其相对含量。结果检出10种成分,鉴定了10种,占挥发油总量的100%。相对含量超过5%的物质有棕榈酸(45.95%)、十六烷酸乙酯(27.91%)、十六烷酸甲酯(8.10%)、油酸乙酯(5.68%)。 To analyze the chemical constituents of volatile oil extracts from Jiangzhining Granules, the volatile oil components were extract- ed and isolated using steam distillation method according to Chinese Pharmacopoeia (2010). The chemical compositions were separated by GC capillary column chromatography, and the relative contents were analyzed by GC-MS. The 10 chromatographic peaks were detected, accounting for 100% of total volatile oil. The compounds that contain more than 5% of the relative contents were: Hexadecanoic acid (45.95%), Hexadecanoic acid, ethyl ester (27.91%), Hexadecanoic acid, methyl ester(8.10%), Ethyl Oleate (5.68%).
出处 《特产研究》 2012年第2期53-54,共2页 Special Wild Economic Animal and Plant Research
关键词 降脂宁颗粒 挥发油 气相色谱-质谱 Jiangzhining Granules Volatile oil GC-MS
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