2,4-二(邻溴苯基)-3-亚胺基丁腈的合成

Synthesis of 2,4-bis (α'-bromophenyl)-3-imido butyronitrile

报道以邻溴苯甲醇为原料，经溴代、氰化及α-负碳离子的亲核加成反应，合成出2，4-二（邻溴苯基）-3-亚胺基丁腈。3步反应收率分别为93％、95％、39％。各步产物结构经IR、MS、NMR分析数据得以确定。

2, 4-Bis (α' -bromophenyl)-3-imido butyronitrile was synthesized by the dipolymerization of a-bromobenzyl cyanide. The product was characterized by IR,NMR and mass spectrometry.