摘要
三嗪类环蕃是一类具有独特性质的超分子主体化合物。用三聚氯氰、1,6-己二胺、4,4'-二氨基二苯醚、4,4'-二氨基二苯甲烷、联苯胺、对苯二胺为原料,合成了一系列三嗪类氮杂环蕃,用十二胺修饰,得标题化合物,并用1HNMR、IR和MALDI-TOF-MS对其结构进行了表征。
Azacyclophanes of 1,3,5-triazine is a kind of supramolecular host compounds,which have some unique characteristics.Several novel soluble azayclophanes were synthesized from dodecylamine and azayclophanes of 1,3,5-triazine.Azayclophanes of 1,3,5-triazine were obtained from reaction of cyanuric chloride with 1,6-hexane diamine,4,4′-diaminodiphenyl ether,4,4′-diaminodiphenyl methane,benzidine and p-phenylene diamine.The structures of the intermediates and the target compounds were confirmed by 1HNMR,IR,MALDI-TOF-MS.
出处
《化学试剂》
CAS
CSCD
北大核心
2012年第7期667-669,共3页
Chemical Reagents
关键词
三聚氯氰
可溶性环蕃
合成
表征
cyanuric chloride
soluble cyclophanes
synthesis
characterization
