摘要
以苄胺和溴代乙酸乙酯为原料 ,干苯为溶剂 ,三乙胺为质子吸收剂 ,合成了 N,N-二乙酸乙酯苄胺 ,产率为 80 %。介绍了该物质的分离纯化方法 ,并用1
In this paper,N,Ndiethylacetate benzylamine has been synthesized from benzylamine and ethyl bromoacetate.The reaction conditions were studied and the structure was characterized by 1HNMR and mass spectra.The yield was 80%.
出处
《化学试剂》
CAS
CSCD
2000年第3期143-144,共2页
Chemical Reagents
关键词
N
N-二乙酸乙酯苄胺
结构表征
合成
苄胺
N,Ndiethylacetate benzylamine
ethyl bromoacetate
triethylamine
proton absorbent
structural characterization