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双-2,3,4-三氟苯脲及其衍生物的合成与表征 被引量：1

Synthesis and Characterization of Di-2,3, 4-trifluorophenylurea and Its Derivatives
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摘要 以不同的取代苯胺和稍过量的固体光气为原料,一锅煮串联反应方便地合成了双-2,3,4-三氟苯脲及其衍生物.产物结构通过IR,1 H NMR,ESI-MS和元素分析表征,并对反应条件和波谱性质进行了讨论。 Starting from different substituted aniline and slightly excess triphosgene,di-2,3,4-trifluorophenylurea and its derivatives were conveniently obtained from one-pot tandem reaction.The structures of the products was characterized by IR,1H NMR,ESI-MS and elemental analysis,and the reaction conditions and spectral properties were discussed.
作者 闫凤美 张燕 李瑞玲
机构地区 黄淮学院化学化工系
出处 《化学世界》 CAS CSCD 北大核心 2012年第8期494-496,500,共4页 Chemical World
基金 河南省基础与前沿技术研究项目(122300410209)
关键词 双-2 3 4-三氟苯脲 衍生物 串联反应 合成 表征 di-2 3 4-trifluorophenylurea derivative tandem reaction synthesis characterization
分类号 O625.63 [理学—有机化学]
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化学世界
2012年 第8期

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