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异丁基硼酸的超声辐射合成 被引量:2

The Ultrasound Irradiation Synthesis of Isobutylbornic Acid
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摘要 在超声条件下,以卤代烃、金属镁粉、硼酸酯为原料合成了异丁基硼酸.反应的最佳条件为:以碘及二溴乙烷做催化剂,超声波功率为175 W,反应时间为15 min,反应温度为40℃. Under the condition of ultrasonic conditions, halogenated hydrocarbon, magnesium powder reacts with boric acid ester giving the product of isobutyl boric acid. The best reaction conditions: iodine, and dibromoethane for catalyst, ultrasonic power for 175 W, reaction time for 15 minutes, reaction temperature for 40 ℃.
出处 《江西师范大学学报(自然科学版)》 CAS 北大核心 2012年第4期415-416,共2页 Journal of Jiangxi Normal University(Natural Science Edition)
基金 国家自然科学基金(81060326) 江西中医学院基金(2009)资助项目
关键词 超声辐射 异丁基硼酸 合成 ultrasound radiation isobutyl boric acid synthesis
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