4,4′-硝基苯基偶磷氮酰苯胺的合成

Synthesis of 4,4'-Nitrophenylphosphagoanliide

在2-甲基吡啶存在下,通过对-硝基苯胺与三氯化磷的作用合成了相应的偶磷氮基化合物。其结构通过IR、HNMR、MS等加以确证。

4, 4'—Nitrophenylphosphajoanilide is synthesiged by means of reaction of p-nitroaniline with trichloride phosphorus in the presence of 2-methyl pyridine. The structure of the title conpound is confirmed by IR,'HNMR,MS.