分散固相萃取—高效液相色谱法测定面包中的丙烯酰胺
摘要
建立了分散固相苹取一高效液相色谱法测定面包中丙烯酰胺的方法。样品以水作提取剂，再用化学方法和分散固相萃取法联合对样品进行纯化，采用高效液相色谱进行分析。该方法的检出限15p,g／kg，线性范围0．05~0．5mg／L，加标回收率85．3％~92．5％，日内精密度RSD为2．9％-5．3％（n=5）；日间精密度RSD为3．6%-10．2%（n=15）。
出处
《农业机械》
2012年第20期87-89,共3页
Farm Machinery
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