摘要
An efficient and novel method for the thioetherification of an alcohol with disulfides or NaSH under microwave irradiation is presented. In the presence of iodine, a variety of alcohols were smoothly S-alkylated with disulfides or NaSH to give the corresponding thioethers in moderate to excellent yields.
An efficient and novel method for the thioetherification of an alcohol with disulfides or NaSH under microwave irradiation is presented. In the presence of iodine, a variety of alcohols were smoothly S-alkylated with disulfides or NaSH to give the corresponding thioethers in moderate to excellent yields.
基金
We thank the National Natural Science Foundation of China （Nos. 21002070 and 21102104）, Zhejiang Pro- vincial Natural Science Foundation of China （No. Y4100307） and the Opening Foundation of Zhejiang Provincial Top Key Discipline （No. 100061200110） for financial support.
