摘要
利用微波水热技术合成CdS半导体纳米晶体,可以克服有机合成方法毒性大,成本高等问题,通过XRD、TEM表征,产物CdS半导体纳米晶体具有立方晶相,纯度较高。通过紫外吸收光谱和荧光光谱分析,发现该方法制备出的半导体CdS纳米晶体具有良好的光致发光性质,证明水相同样适合高质量CdS半导体纳米晶体的生长。
CdS semiconductor nanocrystals（NCs） were synthesized by microwave-hydrothermal method in water solution.In comparison,with the synthesis of NCs in organic solvents,the growth surroundings of aqueous NCs were more poisonous and costly.The XRD and TEM provided direct evidence for a cubic zinc blende structure of bulk CdS crystal.Moreover,the CdS NCs had excellent photoluminescence properties by the characterizations of absorption spectra and luminescence spectra.This method proved that CdS NCs suited to grow in aqueous condition.
出处
《广州化工》
CAS
2012年第22期51-52,80,共3页
GuangZhou Chemical Industry
基金
吉林市科技支撑计划项目(201162506)
关键词
CDS
合成
微波
CdS
preparation
microwave
