期刊文献+

基于近红外光谱和化学计量学方法的灵芝孢子油识别研究 被引量:3

Ganoderma Lucidum Spore Oil Authentication Based on Near-Infrared Spectroscopy Combined with Chemometrics
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摘要 采用近红外透射法建立了一种灵芝孢子油识别方法。分别在灵芝孢子油中掺入葵花油、薏仁油、花生油、玉米油和食用调和油。这些掺杂油品的体积百分比范围为0~100%。采用近红外透射法进行测定。选择最佳的光谱波段,然后用偏最小二乘(Partial Least Squares,PLS)法分别建立了定量分析模型。对于不同比例的掺杂油料,预测相对误差范围在-0.357~0.435之间。研究结果表明,基于化学计量学和近红外光谱技术的分析手段可以作为一种简便、快捷、准确、廉价的方法应用于油类品种识别和掺杂量检测中。 A ganoderma lucidum spore oil authentication method is established by using near-infrared spectroscopy. The sunflower oil, barley oil, peanut oil, corn oil and blend oil are mixed into the ganoderma lucidum spore oil respectively. These mixed oil has a volume percentage from 0 to 100. The near-infrared spectroscopy is used for determination. After the optimal spectral bands are selected, a quantitative analysis model is established by using Partial Least Squares (PLS). The model has a relative prediction error in the range from -0.357 to 0.435 for the mixed oil with different adulterated percentages. The research result shows that this analysis method based on chemometrics and near-infrared spectroscopy is a simple, rapid, low-cost and accurate method for the authentication of oil kinds and the detection of mixer content.
出处 《红外》 CAS 2012年第12期27-32,共6页 Infrared
基金 科技部支撑计划产学研项目(2011BAK10B04) 福建省科技厅重大项目(2011N5008) 福建省科技攻关重点项目(2010Y0001)
关键词 近红外光谱 偏最小二乘法 灵芝孢子油 识别 near-infrared spectrum(NIRS) partial least-squares(PLS) ganoderma lucidum spore oil authentication
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参考文献13

  • 1Cerretani L, Lerma-Garcia M J, Herrero-MartinezJ M, et al. Determination of Tocopherols and To-cotrienols in Vegetable Oils by Nanoliquid Chro-matography with Ultraviolet-visible Detection Usinga Silica Monolithic Column [J]. J Agric Food Chem,2010, 58: 757-761.
  • 2Skrobot V L, Castro E V R, Pereira R C C, et al. Useof Principal Component Analysis (PCA) and Lin-ear Discriminate Analysis (LDA) in Gas Chromato-graphic (GC) Data in the Investigation of GasolineAdulteration [J]. Energy Sz Fuels, 2007, 21: 3394-3400.
  • 3Lerma-Garcia M J, Simo-Alfonso E F, Mendez A,et al. Fast Separation and Determination of Sterolsin Vegetable Oils by Ultraperformance Liquid Chro-matography with Atmospheric Pressure ChemicalIonization Mass Spectrometry Detection [J]. J AgricFood Chem, 2010,58: 2771-2776.
  • 4Mannina L, D’Imperio M, Capitani D, et al. 1HNMR-Based Protocol for the Detection of Adulter-ations of Refined Olive Oil with Refined Hazelnut Oil[J]. J Agric Food Chem, 2009, 57: 11550—11556.
  • 5Say ago A, Garcia-Gonzalez D L, Morales M T, et al.Detection of the Presence of Refined Hazelnut Oil inRefined Olive Oil by Fluorescence Spectroscopy [J].J Agric Food Chem, 2007, 55: 2068—2071.
  • 6Vergara-Barberan M, Escrig-Domenech A, Lerma-Garcia M J, et al. Capillary Electrophoresis of FreeFatty Acids by Indirect Ultraviolet Detection: Ap-plication to the Classification of Vegetable Oils Ac-cording to Their Botanical Origin [J]. J Agric FoodChem, 2011, 59: 10775-10780.
  • 7Zou M, Zhang X,Qi X,et al. Rapid Authenticationof Olive Oil Adulteration by Raman Spectrometry[J]. J Agric Food Chem, 2009, 57: 6001-6006.
  • 8Sanchez-Hernandez L, Nozal L, Marina M L, et al.Determination of Nonprotein Amino Acids and Be-taines in Vegetable Oils by Flow Injection Triple-quadrupole Tandem Mass Spectrometry: A Screen-ing Method for the Detection of Adulterations ofOlive Oils [J]. J Agric Food Chem, 2012,60: 896-903.
  • 9Nicolai B, Beullens K, Bobelyn B, et al. Nondestruc-tive Measurements of Fruit and Vegetable Quality byMeans of NIR Spectroscopy: A Review [J]. Posthar-vest Biol Technol, 2007, 46: 99-118.
  • 10Lin H, Ying Y. Theory and Application of Near In-frared Spectroscopy in Assessment of Fruit Quality:A Review [J]. Sens Instrum Food Qua], 2009, 3: 130-141.

同被引文献23

  • 1唐琼英,柯友胜.导热油特性及使用中若干问题的分析[J].工业加热,2007,36(4):61-64. 被引量:5
  • 2Cerretani L, Lerma-Garcia M J, H errero-M artin ez, J M. et al. Determination of Tocopherols and Tocotrienols in Veg- etable Oils by Nanoliquid Chromatography with Ultraviolet- visible Detection Using a Silica Monolithic Column [J]. J Ag- ric Food Chem. 2010, 58:757 - 761.
  • 3Skrobot V L, Castro E V R Pereira R C C, et al. Use of Principal Component Analysis (PCA) and Linear Discrimi- nate Analysis (LDA) in Gas Chromatographic (G C ) Data in the Investigation of Gasoline Adulteration [J]. Energy & Fuels, 2007, 21: 3394-3400.
  • 4Lerma-Garcia M J, Simo-Alfonso E F, Mendez A, et al. Fast Separation and Determination of Sterols in Vegetable Oils by Ultraperformance Liquid Chromatography with At- mospheric Pressure Chemical Ionization Mass Spectrometry Detection [J]. J Agic Food Chem., 2010, 58:2771-2776.
  • 5Mannina L, D' Imperio M, Capitan i D, et al. 1H NMR Based Protocol for the Detection of Adulte rations of Re- fined Olive Oil with Refined Hazelnut Oil [J]. J Agric FoodChem. 2009.5 7 : 11550-11556.
  • 6Sayago A, Garcia-Gonzalez D L, Morales M T, et al, De- tection of the Presence of Refined Hazelnut Oil in Refined Olive Oil by Fluorescence Spectroscopy [J]. J Agric Food Chem, 2007, 55:2068-2071.
  • 7Vergara-Barberan M, Escrig-D om enech A, LermaGarcia M J, et al. Capillary Electrophoresis of Free Fatty Acids by Indirect Ultraviolet Detection: Application to the Classifica- tion of Vegetable Oils According to Their Botanieal Origin [J]. J Agile Food Chem, 2011, 59, 10775-10780.
  • 8Zou M Q, Zhang X F, Qi X H, et al. Rapid authentication of olive oil adulteration by Raman spectrometry[J]. Journal of agricultural and food chemistry, 2009, 57 (14): 6001- 6006.
  • 9Sanchez-Hernandez L, NozalL, Marina M L, et al. Deter- mination of Nonprote in Amino Acids and Betaines in Vege- table Oils by Flow Injection Triplequadrupole Tandem Mass Spectrome try: A Screening Method for the Detection of Adulterations of Olive Oils. [J] J. Agric Food Chem. 2012, 60:896-903.
  • 10Lin H, Ying Y. Theory and application of near infrared spec- troscopy in assessment of fruit quality: a review[J]. Sensing and instrumentation for food quality and safety, 2009, 3 (2): 130-141.

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