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微波促进5-芳亚甲基罗丹宁化合物的合成及晶体结构 被引量：2

Synthesis of 5-arylalkylidenerhodanines under microwave irradiation and crystal structure
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摘要 以芳香醛和罗丹宁为原料,在乙酸钠/乙酸体系中经微波辐射反应得到一系列5-芳亚甲基罗丹宁,化合物结构经1H NMR和红外光谱确证。并对5-(4-硝基苯亚甲基)罗丹宁/四氢呋喃单晶进行了解析。 A series of 5-arylalkylidenerhedanines were synthesized by the Knoevenagel condensation of aromatic aldehyde with rho- danine in sodium acetate/acetic acid under microwave irradiation. The structures of products were characterized by ^1H NMR and IR spectra. Furthermore,the structure of 5-（4＇nitmbenzylidene）rhodanine/THF was determined by X-ray single crystal diffraction.
作者 蒋军荣 徐峰 柯中炉
机构地区 台州职业技术学院生化制药研发中心
出处 《化学研究与应用》 CAS CSCD 北大核心 2012年第12期1836-1839,共4页 Chemical Research and Application
基金 台州职业技术学院科研项目(2010ZD09)资助
关键词 微波 芳亚甲基罗丹宁 晶体结构 合成 microwave arylalkylidenerhodanines crystal structure synthesis
分类号 O626.2 [理学—有机化学]
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参考文献12

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二级参考文献35

共引文献19

同被引文献24

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化学研究与应用
2012年 第12期

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