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一种简易的硫化亚锡微米棒薄膜的合成

A facile synthesis of SnS microrods films
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摘要 为了得到高纯度的硫化亚锡薄膜,利用恒电压法成功制备了硫化亚锡微米棒薄膜,并将该薄膜在200℃真空退火1 h.结构和形貌分析表明:该薄膜是由2～5μm的细棒组成,并且优先沿着(101)晶面方向生长.拉曼光谱表明该薄膜具有较高的纯度. In order to get SnS with high purity, the SnS microrods films were prepared by constant potential cathodic electro-eposition method and annealed at 200 ℃ under vacuum conditions for 1 h. The structure and morphology analysis showed the films were composed of micro-sized rods. The length of the rods was in a range of 2 - 5 micro and preferentially oriented along the （ 101 ） plane. Raman spectra indicated that the microrods films had a high purity.
作者 杜元宝 韩聪 蔡嫦芳 孟庆哲 孟秀清 吴锋民
机构地区 浙江师范大学LED芯片研发中心
出处 《浙江师范大学学报（自然科学版）》 CAS 2013年第1期65-67,共3页 Journal of Zhejiang Normal University:Natural Sciences
基金 浙江省自然科学基金资助项目(Z6090556) 浙江省新苗人才计划孵化项目(4053)
关键词 微米棒 乙二胺四乙酸(EDTA) 恒电压法 温度退火 microrods EDTA constant potential cathodic method temperature anneal
分类号 O646.54 [理学—物理化学]
  • 相关文献

参考文献12

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二级参考文献29

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浙江师范大学学报（自然科学版）
2013年 第1期

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