摘要
目的:采用高效液相色谱法建立了一种全面控制止嗽定喘丸(浓缩丸)内在质量的方法。方法:以混合对照药材作为对照,对处方中全部药味进行定性鉴别。结果:4批样品均呈现与混合对照药材色谱保留时间一致的主要特征峰,各味药材不相互干扰。结论:本方法重复性好,操作简便,可作为止嗽定喘丸(浓缩丸)的质量控制方法。
Objective: To establish a comprehensive method for the quality control of Zhisou Dingchuan Pills by HPLC. Methods: All herbs in prescription were identified by compare with the chromatogram of mixed reference crude herb. Results: 4 samples were presented main peaks with same retention time with the chromatograrn of mixed reference crude herb, and the peaks did not interfere with each other. Conclusion: The validated method was applied for 4 batches of samples, which proved to be reproducible, convenient and could be used as quality control methed for Zhisou Dingchuan Pills.
出处
《中华中医药杂志》
CAS
CSCD
北大核心
2013年第2期538-540,共3页
China Journal of Traditional Chinese Medicine and Pharmacy
基金
国家药品标准提高研究项目(No.09-204)
河北省自然科学基金-石药集团医药联合研究基金(No.C2011320007)~~