摘要
制备了锆(Ⅳ)与乙酰丙酮(HAA)、三氟乙酰丙酮(HTFA)、二苯甲酰甲烷(HDBM)等的MA_4型配合物,研究了它们的合成条件,熔点等基本性质以及它们在4000～250cm^(-1)
Reported herein is the preparation and properties of the tetrakis β-diketonates of zirconium (IV) with acetylacetone, dibenzoyl-methane, and trifiuoroacetylacetone.
The methods of preparing the complexes are discussed. The essential characterization as their melting points and their infrared spectra are observed in 4 000-250 cm-1 range.
出处
《北方工业大学学报》
1991年第3期10-15,共6页
Journal of North China University of Technology
关键词
锆
配合物
Β-二酮
合成
β-diketonato complexes, zirconium complex, differential thermo-analysis,infrared spectra
