摘要
本文系统地研究了棉籽油脱臭馏出物中甾醇提取方法,主要得出以下结论:采用转酯化-结晶法对棉籽油脱臭馏出物中甾醇进行萃取,最佳萃取条件为:料液比为1/5(m/V),转酯化温度为60℃,催化剂使用量为35%,转酯化时间为4 h,甾醇提取率为54.80%,甾醇纯度达到82.10%。
A process for extracting plant sterol fi'om cotton oil deodorizer distillate and the crystal purification were studied. The optimal conditions for transesterification of sterol ester were obtained as followed: the rate of blend composition 1/5 (m/V ), temperature 60 ℃, the dosage of catalyst 35% and time 4.0 hour. The recovery rate was 54.8% and purity of rough sterol was 82.10%.
出处
《现代食品科技》
EI
CAS
北大核心
2013年第3期568-570,493,共4页
Modern Food Science and Technology
基金
国家大学生创新性实验计划项目(101075925)
关键词
脱臭馏出物
甾醇
高效液相色谱法
deodorized soybean oil
phytosterol
high efficiency liquid chromatography