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3-环丙基-3-氧代丙酸甲酯的合成工艺改进

Improved Synthesis of 3-Cyclopropyl-3-oxopropionic Acid Methyl Ester
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摘要 本研究以环丙甲酮、碳酸二甲酯为原料在氢化钠的存在下合成了3-环丙基-3-氧代丙酸甲酯,改进后的工艺反应周期短,成本低廉,收率达到86.5%,适合于工业化生产。 3-Cyclopropyl-3-oxopropionic acid methyl ester was prepared from Cyclopropyl methyl ketone and dimethyl carbonate in the presence of sodium hydride. The method was improved for industrial production and the product was obtained in 86.5 % yield.
作者 徐斌 程锦涛
机构地区 台州市知青化工有限公司
出处 《广东化工》 CAS 2013年第6期50-51,共2页 Guangdong Chemical Industry
关键词 3-环丙基-3-氧代丙酸甲酯 合成 工艺改进 J3-Cyclopropyl-3-oxopropionic acid methyl estcr synthesis： process improvement
分类号 TQ560.6 [化学工程—炸药化工]
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参考文献8

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二级参考文献6

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共引文献8

广东化工
2013年 第6期

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