摘要
应用1DNMR和梯度2DNMR反相技术（gCOSY，gNOESY，gHMQC，gHMBC）研究了从疏毛吴茱萸中分离得到的三个生物碱：吴茱萸碱、吴茱萸次碱和去氢吴茱萸碱的结构，并对其碳氢NMR信号进行了全归属．
Three alkaloids, Evodiamine, Rutaecarpine and Dehydroevodiamine, were isolated fromthe fruits of Evndia rutaecarpa (Juss) var. bodinaieri (Dode) Huang. In this paper, all ofthe iH and 13C NMR chemical shifts of these compounds were assigned through iD NMRand 2D NMR with Pulse Field Gradient (PFG) techniques (gCOSY, gNOESY, gHMQC andgHMBC).
出处
《波谱学杂志》
CAS
CSCD
北大核心
1999年第6期563-568,共6页
Chinese Journal of Magnetic Resonance
基金
国家"九五"科技攻关资助!96-901-01-39
关键词
吴茱萸碱
吴茱萸次碱
云氢吴茱萸碱
NMR
中药
Endia rutaecarpa (Juss) Benth var. bodinaieri, Evodiamine, Rutaecarpine, Dehydroevodiamine, 2D NMR with Pulse Field Gradient (PFG)
