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ZrB2-SiC超高温陶瓷的定量分析

Quantitative Phase Analysis of The ZrB_2-SiC Ultrahigh Temperature Ceramics
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摘要 利用XRD对超高温陶瓷粉进行分析,从衍射谱图能得到各物相组成为ZrB2、SiC、ZrO2,并且采用全谱拟合法对各物相进行定量计算。结果显示,定量分析结果的绝对误差小于2%,全谱拟合分析方法能准确地对超高温陶瓷的物相进行定量分析。 The phase composition of ZrB2-SIC ultrahigh temperature ceramics （UTC）are analyzed by XRD, and the quantitative analysis data were obtained from the Rietveld analyses. The results show that the phase compositions of UTC are ZrB/, SiC, ZrO2, the quantitative analysis data from this work are close to the real ratio of the samples. The Rietveld methord is reliable for the quantitative phase analysis of the ZrB2-SiC ultrahigh temperature ceramics.
作者 王晓叶 郑斌 冯志海
机构地区 航天材料及工艺研究所
出处 《宇航材料工艺》 CAS CSCD 北大核心 2013年第2期95-98,共4页 Aerospace Materials & Technology
关键词 高温陶瓷 X射线衍射 全谱拟合法 物相定量 ZrB2--SiC Ultrahigh temperature ceramic, X-ray diffraction, Rietiveld methord, Quantitative analysis, ZrB2-SIC
分类号 V254.2 [一般工业技术—材料科学与工程]
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参考文献12

  • 1Fahrenholtz W G, Hilmas G E. NSF-AFOSR joint workshop on future ultra-high temperature materials [ R ]. NSF Grant DMR-0403004.
  • 2Upadhya K,Yang J M,Hoffmann W P. Materials for ultra-high temperature structural applications [ J ]. Am. Ceram. Soc. Bull, 1997,76(12) :51-56.
  • 3韩杰才,胡平,张幸红,孟松鹤.超高温材料的研究进展[J].固体火箭技术,2005,28(4):289-294. 被引量：58
  • 4Bronson A, Ma Y T, Mutso R. Compatibility of refractory metal borider/oxide composites at ultra-high temperature [ J ]. Electrochem. Soc. , 1992,139 ( 11 ) : 3183-3196.
  • 5萨姆索洛夫,难熔化合物手册[M].北京:中国工业出版社,1965:145-289.
  • 6Levine S R, Opila E J, Halbig M C, et al. Evaluation of ultra-high temperature ceramics for aeropropulsion use [ J ]. Europe Ceram Society,2002,22( 14/15 ) :2757-2767.
  • 7Opeka M M, Talmy I G, Zayko J A. Oxidation-based materials selection for 2000℃ hypersonic aerosurfaces, theoretical considerations and historical experience [ J ]. Material Science, 2004,39(19) :5887-5904.
  • 8Tripp W C, Davis H H, Graham H C. Effect of a SiC addition on the oxidation of ZrB2 [ J ]. Ceram. Bull. , 1973,52 (8) :612-616.
  • 9于军,章徳铭,杨永琦,刘建明,任先京.超高温陶瓷材料的研究[J].热喷涂技术,2011,3(1):29-33. 被引量：9
  • 10李树堂.晶体X射线衍射学基础[M].北京：冶金工业出版社,1990.116-138.

二级参考文献69

  • 1韩杰才,胡平,张幸红,孟松鹤.超高温材料的研究进展[J].固体火箭技术,2005,28(4):289-294. 被引量：58
  • 2Upadhya K,Yang J-M,Hoffmann W P. Materials for ultrahigh temperature structural applications [ J ]. Am. Ceram.Soc. Bull, 1997,76(12) :51-56.
  • 3William G Fahrenholtz,Gregory E Hilmas. NSF-AFOSR joint workshop on future ultra-high temperature materials [ R].NSF Grant DMR-0403004.
  • 4Bronson A, Ma Y T, Mutso R. Compatibility of refractory metal boride/oxide composites at ultra-high temperatures[J]. J. Electrochem. Soc. ,1992,139( 11 ) :3183-3196.
  • 5Opeka M,Talmy I G, Wuchina E J, Zaykoski J A, Causey S J. Mechanical, thermal, and oxidation properties of refractory hafnium and zirconium compounds [ J ]. J. Eur. Ceram. Soc. ,1999,19(13-14) :2405-2414.
  • 6Wang C R, Yang J M, Hoffmann W. Thermal stability of refractory carbide/boride composites [ J ]. Mater. Chem. Phys.,2002,74 ( 3 ): 272-274.
  • 7Hinze J W,TrippW C, Graham H C. High-temperature oxidation behavior of a HfB2 plus 20 v/o SiC composite [ J ]. J.Electrochem. Soc. , 1975,122(9): 1249-1254.
  • 8Tripp W C, Davis H H, Graham H C. Effect of an SiC addition on the oxidation of ZrB2 [ J ]. Ceram. Bull, 1973,52(8) :612-616.
  • 9Levine S R, Opila E J, Halbig M C, Kiser J D, Singh M, Salem J A. Evaluation of ultra-high temperature ceramics for aeropropulsion use [ J ]. J. Eur. Ceram. Soc. , 2002,22 ( 14,15 ) :2757-2767.
  • 10Opeka M M, Talmy I G, Zaykoski J A. Oxidation-based materials selection for 2000℃ + hypersonic aerosurfaces:Theoretical considerations and historical experience [ J ]. J. Mater.Sci. ,2004,39 (19): 5887-5904.

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