大黄灌肠液的薄层色谱鉴别方法及土大黄苷的限量检查方法

Limit test method of rhubarb enema TLC method and soil solution of rhubarb aglycone

目的:建立大黄灌肠液的薄层色谱鉴别方法及土大黄苷的限量检查方法。方法:采用薄层色谱鉴别方法鉴别大黄灌肠液中的主要成分大黄及土大黄苷的限量检查。结果:所建立的大黄灌肠液中的大黄薄层鉴别方法阴性对照无干扰,专属性强,斑点清晰,操作简单;土大黄苷限量检查简单易行。结论:可作为大黄灌肠液的质量标准的部分内容。

Objective：To establish rhubarb enema TLC identification and Rumex glycosides limited inspection methods. Methods：The main ingredient TLC identification method to identify rhubarb enema rhubarb and soil rhubarb aglycone limited check. Results：Established rhubarb enema TLC method negative control without interference,specific and clear spots,simple operation; Rumex glycosides limited screening is simple. Conclusion：As a part of the contents Rhubarb Enema quality standard.