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Comparative TEM investigation on the precipitation behaviors in Cu-15wt% Sn alloy 被引量:2

Comparative TEM investigation on the precipitation behaviors in Cu–15wt% Sn alloy
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摘要 The decomposition and precipitation behaviors of a quenched Cu-15wt%Sn alloy as a function of aging temperature were investigated using transmission electron microscopy (TEM). Focused ion beam (FIB) was employed to assist TEM specimen preparation. At 300 ℃, the decomposition of the supersaturated phase occurred at grain boundaries, displaying a cellular morphology. The lamellae were found with and phases, rather than with the equilibrium e and phases. The and phases exhibit a welldefined orientation relationship (OR) as On the other hand, at 320 ℃, only incipient lamellar structures of several micron meters were observed, which were composed of the 6 and phases. At the same time, abundant intragranular precipitation of the e phase in the form of platelets was observed, and OR as (lil)J/ (001), [110] J/[100] exists between e phase and the ct phase. These contrasting precipitation behaviors are discussed from the viewpoint of crystallographic coherency of these phases. The decomposition and precipitation behaviors of a quenched Cu-15wt%Sn alloy as a function of aging temperature were investigated using transmission electron microscopy (TEM). Focused ion beam (FIB) was employed to assist TEM specimen preparation. At 300 ℃, the decomposition of the supersaturated phase occurred at grain boundaries, displaying a cellular morphology. The lamellae were found with and phases, rather than with the equilibrium e and phases. The and phases exhibit a welldefined orientation relationship (OR) as On the other hand, at 320 ℃, only incipient lamellar structures of several micron meters were observed, which were composed of the 6 and phases. At the same time, abundant intragranular precipitation of the e phase in the form of platelets was observed, and OR as (lil)J/ (001), [110] J/[100] exists between e phase and the ct phase. These contrasting precipitation behaviors are discussed from the viewpoint of crystallographic coherency of these phases.
出处 《Rare Metals》 SCIE EI CAS CSCD 2013年第2期139-143,共5页 稀有金属(英文版)
基金 supported by the China Scholarship Council(No.2010602038) the Ministry of Science and Technology of China(No.2010DFA51650)
关键词 Cu-Sn alloy Precipitation behaviorsFocused ion beam (FIB) TEM CRYSTALLOGRAPHY Cu-Sn alloy Precipitation behaviorsFocused ion beam (FIB) TEM Crystallography
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