摘要
通过水热法合成了2个新的金属-有机配位聚合物[Pb(NA)L]n1,[Pb(CH3COO)L]n.nH2O 2(H2NA=烟酸,L=2-(4-硝基苯酚基)-1H-咪唑[4,5-f][1,10]邻菲罗啉)。并对其进行了元素分析、红外光谱、热重和X-射线单晶衍射测定。这2个配合物通过氢键和π-π相互作用形成了三维超分子网状结构。此外还研究了配合物1和2的荧光性质。
Two new metal-organic coordination polymers [Pb(NA)L]n 1, [Pb(CH3COO)L]n·nH2O 2 (H2NA=nicotinic acid, L=2-(4-nitrophenol)-1H-imidazo[4,5-f][1,10]phenanthroline) have been hydrothermally synthesized and structurally characterized by elemental analysis, IR, TG and single-crystal X-ray diffraction. They are further extended into a three-dimensional supramolecular network structure through hydrogen-bonding and π-π interactions. Moreover, the luminesent property of 1 and 2 have been investigated in the solid state. CCDC: 931504, 1; 931505, 2.
出处
《无机化学学报》
SCIE
CAS
CSCD
北大核心
2013年第6期1243-1248,共6页
Chinese Journal of Inorganic Chemistry
基金
吉林省教育厅科学技术研究(吉教科合字[2012]第358号)资助项目
关键词
水热合成
晶体结构
铅配合物
hydrothermal synthesis
crystal structure
lead complex