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HPLC-DAD-ESI-MSn和GC-MS比较陈皮、橘皮和霉变橘皮中的化学成分 被引量:10

Comparative analysis on the chemical components of pericarpium Citri Reticulatae,citrus peels and fermented citrus peels with HPLC-DAD-ESI-MSn and GC-MS
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摘要 橘皮是陈皮的原料,很容易感染指状青霉而发生霉变。文中运用HPLC-DAD-ESI-MSn和GC-MS技术分析了陈皮、橘皮以及霉变橘皮中化学成分,比较了三者的总黄酮和总多酚的含量。结果表明:陈皮、橘皮以及霉变橘皮中的非挥发性成分很相似,但是挥发性成分差别很大,同时它们的总黄酮和总多酚含量也不同。柑橘种植过程中使用的杀虫剂,在霉变橘皮中却没有检出。 The peel of Citrus Reticulatae is the raw material of Pericarpium Citri Reticulatae(PCR) , which was easily molded by Penicillium digitatum. The differences of chemical components among Citrus peels (CP) , PCR and molded Citrus peels (FCP) were studied by HPLC-DAD-ESI-MSn and GC-MS. In addition, the total flavonoids and polyphenols were also evaluated in different samples. The results showed that the nonvolatile compounds of CP, PCR and FCP peels were similar, but the volatile compounds of these samples varied significantly. The contents of total flavonoids and polyphenols were significantly different among these samples. In molded samples, the pesticides were not able to detect.
出处 《食品与发酵工业》 CAS CSCD 北大核心 2013年第4期192-199,共8页 Food and Fermentation Industries
基金 国家自然科学基金项目(31201335) 安徽省自然科学基金项目(1308085QC51)
关键词 HPLC-DAD-ESI-MSn GC-MS 黄酮类化合物 霉变 HPLC-DAD-ESI-MSn, GC-MS, flavonoids, mildew
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  • 1Ortuno A, Diaz L,Alvarez Net al. Comparative study of flavonoid and scoparone accumulation in different Citrus species and their susceptibility to Perricillittm digitattm [J]. Food Chemistry,2011,125(1) :232 -239.
  • 2Barreca D, Bellocco E, Caristi C et al. Distribution of C- and O-glycosyl flavonoids, (3-hydroxy-3-methylglutaryl) glycosyl flavanones and furocoumarins in Citrus aurantium L. juice [J]. FoodChemistry,2011,124(2): 576 -582.
  • 3Dugo P,Lo Presti M, Ohman Met al. Determination of fla- vonoids in Citrus juices by micro-HPLC-ESI/MS [ J 1. Journal of Separation Science, 2005, 28 ( 11 ) : 1 149 - 1 156.
  • 4Kim GN, Shin JG, Jang HD activity of Dangyuja (Citrus Antioxidant and antidiabetic grandis Osbeck) extract trea- ted with Aspergillus saitoi [ J ]. Food Chemistry, 2009,117 (1): 35-41.
  • 5Zheng G,Yang D,Wang D et al. Simultaneous Determina- tion of Five Bioactive Flavonoids in Pericarpium Citri Re- ticulatae from China by High-Performance Liquid Chroma- tography with Dual Wavelength Detection [ J]. Journal of Agricultural and Food Chemistry ,2009,57 ( 15 ) 6 552 - 6 557.
  • 6Wang DD, Wang J, Huang XH et al. Identification of polymethoxylated flavones from green tangerine peel ( Peri- carpium Citri Reticulatae Viride) by chromatographic and spectroscopic techniques [ J] . Journal of Pharmaceutical and Biomedical Analysis ,2007,44( 1 ) : 63 - 69.
  • 7Singleton VL, Joseph A, Rossi JR. Colorimetry of Total Phenolics with Phosphomolybdic-Phosphotungstic Acid Re- agents [ J ]. American Journal of Enology and Viticul- ture. 1965.16 : 144 - 158.
  • 8Kim HG, Kim GS, Lee JH et al. Determination of the change of flavonoid components as the defence materials of Citrus unshiu Marc. fruit peel against Penicillium digita- turn by liquid chromatography coupled with tandem mass spectrometry [ J ]. Food Chemistry, 2011,128 ( 1 ) : 49 - 54.
  • 9Wang AY, Zhou MY, Lin WC. Antioxidative and anti-in- flammatory properties of Citrus sulcata extracts [ J ]. Food Chemistry,2011,124(3) : 958 -963.
  • 10Zhang JY,Li N,Che YY et al. Characterization of seventy polymethoxylated flavonoids (PMFs) in the leaves of Murraya paniculata by on-line high-performance liquid chromatography coupled to photodiode array detection and electrospray tandem mass spectrometry [ J ]. Journal of Pharmaceutical and Biomedical Analysis, 2011 , 56 (5) : 950 - 961.

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