双苯乙酮亚胺硫脲Cu(Ⅰ),Zn(Ⅱ),Fe(Ⅱ)配合物的直接电化学合成

The direct electrochemical synthesis of Cu(Ⅰ),Zn(Ⅱ),Fe(Ⅱ) complexes of 1,5-bis(acetophenone) thiocarbohydrazone

用电化学金属阳极氧化法在非水溶剂中合成了苯乙酮双缩硫代对称二氨基脲 (HL)与Cu(Ⅰ ) ,Zn(Ⅱ ) ,Fe(Ⅱ )的配合物 ,通过元素分析、红外光谱、紫外光谱、磁化率、摩尔电导等对配合物进行了表征 .

Cu(I), Zn(II), Fe(II) complexes of 1,5 bis(acetophenone) thiocarbohydrazone were synthesized by the electrochemical oxidation of anodic metal in non aqueous solution. The complexes were characterized by elemental analysis, IR, UV, magnetic measurement and molar conductivity.