摘要
采用GC-MS法分析骨折挫伤胶囊的挥发油化学成分。采用水蒸气蒸馏法提取骨折挫伤胶囊的挥发油,用气相色谱-质谱联用技术对化学成分进行鉴定,以毛细管柱进行分析,面积归一化法测定其相对含量。分离得8个化学组分峰,并确定出其中7个化学成分,占挥发油总数的97.04%。相对含量超过5%的成分有棕榈酸(70.01%)、亚油酸乙酯(9.39%)和Z,Z-亚油酸甲酯(8.31%)。骨折挫伤胶囊中挥发油成分主要包含棕榈酸乙酯、Z,Z-亚油酸甲酯和棕榈酸等成分。
To analyze the chemical constituents of volatile oil extracted from Fracture bruise capsule with GC-MS.Volatile oil was extracted by water-steam distillation.The components were identified by GC-MS and quantitatively determined with normalization method.Eight compounds were separated by GC and 7 of them were identified,accounting for 97.04% of the total volatile oil.The compounds that the relative content was more than 5% were n-Hexadecanoic acid(70.01%),9,12-Octadecadienoic acid,ethyl ester(9.39%),9,12-Octadecadienoic acid(Z,Z)-,methyl ester(8.31%).The maincomponents in the volatile oil of Fracture bruise capsule were n-Hexadecanoic acid,9,12-Octadecadienoic acid,ethyl ester,ethyl ester and 9,12-Octadecadienoic acid(Z,Z)-,methyl ester.
出处
《特产研究》
2013年第2期54-56,共3页
Special Wild Economic Animal and Plant Research