三高调和丸质量标准研究

Studies on the standard quarlities of San Guao Tiao He Wan

目的完善三高调和丸的质量标准。方法采用薄层色谱法(TCL)对处方中的丹参、三七这两种主要药材进行定性鉴别;用高效液相色谱法(HPLC)测定丹参含量。结果 TLC色谱中斑点清晰,易于识别;HPLC法精密度、重现性良好;丹参线性范围0.04032～0.8064μg(r=0.9999);平均回收率为99.5%。结论本法可有效控制三高调和丸的质量。

Objective To improve the standard for the quality control of San Guao Tiao He Wan. Methods Adopt Thin Layer Chromatography （TLC） to identify its Chinese medicine such as Danshen root, notoginseng. Results TLC was a simple, reliable and specific method with good reproducibility, it accords with the demands of pharmacopoeia. HPLC method was precision, reproducibility well; the linear range of Salvia was from 0. 04032 to O. 8064 pg （ r = 0. 9999 ） xbith an average recovery of 99. 5%. Conclusion These methods can be conducive to the improvement and control of the quality of Sangao Tiaohe Wan.