2-水杨酰亚肼基-1,3-二硫杂环戊烷的合成研究

Study of Synthesis on 2 - Salicylic Hydrazono - 1,3 - Dithiolane

以水杨酸甲酯为原料,采用均匀设计优化工艺条件,经两步合成出一种新化合物—2-水杨酰亚肼基-1,3-二硫杂环戊烷。利用元素分析和光谱手段证明其符合预期结构。

A new compound 2 - salicylic hydrazono -1,3- dithiolane is synthesized with methyl salicylat as the starting material Via two steps of reactions under conditions iptimized by use of uniform design. The sturcture of the product was confirmed by elementary analysis and spectrum analysis