摘要
以2,4-二氯苯丁酮为起始原料,经过环合、重排、还原、磺化、缩合5步制得杀菌剂1-[2-(2,4-二氯苯基)戊基]-1H-1,2,4-三唑,总收率达到了67%。
1-[2-(2,4-Dichlorophny)pentyl]-1H-1,2,4-triazole(Penconazole) was prepared in overall yield of 67% via cyclization,rearrangement,reduction,sulfonation and condensation starting from 2,4 dichlorobutyrophenone.
出处
《精细化工中间体》
CAS
2013年第3期18-19,32,共3页
Fine Chemical Intermediates
关键词
戊菌唑
2
4-二氯苯丁酮
合成
penconazole
2
4-Dichlorobutyrophenone
synthesis