高品质1,3,5-三烯丙基-均三嗪-2,4,6-三酮的合成与测试表征

Synthesis and Characterization of High Quality Triallyl Isocyanurate

三烯丙基异氰脲酸酯(TAIC)是一种用途广泛的精细化工产品。笔者以氰尿酸和氯丙烯为起始原料,主要研究了TAIC的合成、提纯和测试表征。TAIC的合成采用二步法,粗产物通过分步提纯后,气相色谱(GC)测试纯度>99.5%。结合对产物、样品TAIC和样品三聚氰酸三烯丙酯(TAC)的熔点、气相色谱(GC)、核磁(13C NMR)和红外(FT-IR)测试分析比较,以及有机化合物图库(SDBS)数据比较,其结果显示合成产物即TAIC。

Triallyl isocyanurate（TAIC） is a fine chemical with wide applications.This paper introduced the synthesis,purification and characterization of high quality of TAIC by using cyanuric acid and allyl chloride as the starting materials.The product was identified with GC,melting point,^13C NMR and FTIR spectra.