参柴调理丸的质量标准研究

Studies on Quality Standard of Shenchai Tiaoli Pills

目的:建立以参柴调理丸的质量标准。方法:采用TLC法对制剂中川芎、牡丹皮、黄芪、人参进行定性鉴别;采用HPLC法测定丹皮酚的含量。结果:薄层鉴别的色谱斑点清晰,阴性对照无干扰。丹皮酚在69.5～1112 ng范围内呈良好的线性关系,平均回收率为100.30%,RSD=1.29%(n=6)。结论:所建立的方法简便可行,专属性强,重复性好,可用于参柴调理丸的质量控制。

Objective ： To establish the quality control menthods for Shenchai Tiaoli pills. Method： The method of TLC was used to identify Rhizoma chuanxiong, Cortex Moutan, Radix Astragali, Radix et Rhizoma Ginseng. The content of pae- onol was determined by HPLC. Results ： The herbal drugs were well identified dy TLC, the spots were clear and without in- terference. The linear range of paeonol was from 69.5ng to 1112ng. The average recovery of paeonol was 100.30%, and the RSD was 1.29% （n = 6）. Conclusion ：The estbablished method is simple and feasible, and can be used as the quality control standard of Shenchai Tiaoli pills.